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• W2067540857 abstract "Two new molybdenum phosphate complexes, [Cu2(phen)4(μ-Cl)][PMo12O40]·H2O (phen = 1,10-phenanthroline) (1) and (Hbpy)[CuI(bpy)]2[PMoV2MoVI10O39] (bpy = 4,4′-bipyridine) (2), have been prepared under mild hydrothermal conditions and structurally characterized by single-crystal X-ray diffraction. Compounds 1 and 2 crystallize in triclinic system, space group , with a = 12.5458(7) Å, b = 13.4486(8) Å, c = 21.2406(12) Å, α = 99.7020(10)°, β = 94.2320(10)°, γ = 95.0890(10)°, V = 3504.2(3) Å3 and Z = 2 for 1, and a = 10.7871(6) Å, b = 10.9016(6) Å, c = 12.7897(7) Å, α = 96.8500(10)°, β = 110.0850(10)°, γ = 103.5800(10)°, V = 1339.74(13) Å3 and Z = 1 for 2. Compound 1 contains a [Cu2(phen)4(μ-Cl)]3+ cation in which two similar [Cu(phen)2] units are bridged by one chlorine atom. Compound 2 contains one-dimensional straight chain of Keggin polyoxoanions [PMoV2MoVI10O39]n3− and two linear cationic chains of [CuI(bpy)]nn+. The molecular packing shows a two-dimensional network, which is formed by the cross of the linear Keggin anions and Cu-bpy cations." @default.
• W2067540857 created "2016-06-24" @default.
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• W2067540857 date "2006-01-01" @default.
• W2067540857 modified "2023-10-17" @default.
• W2067540857 title "Hydrothermal Synthesis and Structures of Two New Molybdenum Phosphate Compounds based on Keggin Cluster Units" @default.
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• W2067540857 doi "https://doi.org/10.1002/zaac.200500357" @default.
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