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- W191106373 abstract "Publisher Summary This chapter discusses the modified synthesis of 1-deoxyald-l-enopyranose (2-hydroxyglycal) esters. The hydroxyglycal esters, more systematically described as esters of 1-deoxyald-l-enopyranoses, are well-known compounds prepared by the elimination of the elements of hydrogen halide from acylated glycosyl halides. An alternative modification involves the conversion of glycosyl bromides to iodides prior to the eliminations. Esters of 1-deoxyald-l-enopyranoses can also be converted to 2,3-unsaturated glycopyranosides by treatment in benzene solution with alcohols in the presence of boron trifluoride etherate. In the glycal (1,2-dideoxyald-l-enopyranose) series, rearrangement reactions can be effected similarly, and in particular, 4,6-di-O-acetyl-2,3-dideoxy-α- d -erythro-hex-2-enopyranosides can be synthesized from tri-O-acetyl- d -glucal." @default.
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- W191106373 date "1972-01-01" @default.
- W191106373 modified "2023-09-26" @default.
- W191106373 title "Modified Synthesis of 1-Deoxyald-1-enopyranose (2-Hydroxyglycal) Esters" @default.
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- W191106373 doi "https://doi.org/10.1016/b978-0-12-746206-6.50061-8" @default.
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