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• W1967051722 abstract "Abstract In present work, thermal properties of silver thiogallate (AgGaS 2 ) crystal were investigated by means of differential scanning calorimetry (DSC) measurements performed at different heating and cooling rates. The DSC results confirmed that the melting point was 1249 K with a slight change around 5 K and that the nucleation temperature varied from 1183 K to 1218 K. The supercooling temperature was evaluated in the range 37.69 K to 62.46 K which was considered to be harmful for the single nucleus formation at the beginning of crystal growth. The activation energy E and the pre-exponential factor A were also calculated using different isoconversional methods, namely Kissinger–Akahira–Sunose (KAS) method and Flynn–Wall–Ozawa (FWO) method, and the results showed good agreement with each other. According to the results of DSC, a larger temperature gradient up to 30 K/cm was utilized to suppress the formation and growth of multi nuclei and a rapid cooling rate 25 K/min was applied to minimize the second-phase precipitates during the process of crystal growth. Finally, an integral and transparent AgGaS 2 single crystal with diameter of 22 mm and the length of 55 mm was obtained." @default.
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• W1967051722 date "2014-09-01" @default.
• W1967051722 modified "2023-09-29" @default.
• W1967051722 title "Thermal properties and optimization of process parameters for the growth of silver thiogallate crystal by differential scanning calorimetry" @default.
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• W1967051722 doi "https://doi.org/10.1016/j.jcrysgro.2014.04.032" @default.
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