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- W1970512935 abstract "Abstract The reductive metallation of the readily available peracetylated derivatives of methyl N ‐acetylneuraminate 3a and 3b by samarium diiodide without any additive generates the corresponding anomeric samarium(III) organometallics. These intermediates react efficiently with carbonyl compounds under Barbier conditions, providing a fast synthesis of C ‐ketosides. The α‐ and β‐acetates are equally effective, and excellent yields are obtained for coupling with cyclic ketones. The procedure has been conveniently applied to the synthesis of a C ‐ketoside of N ‐acetylneuraminic acid with an attached linker, ready to use as a building block in the elaboration of multivalent biological probes. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2007)" @default.
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- W1970512935 date "2007-06-18" @default.
- W1970512935 modified "2023-10-10" @default.
- W1970512935 title "An Expeditious Synthesis of <i>N</i>‐Acetylneuraminic Acid α‐<i>C</i>‐Glycosyl Derivatives (“α‐<i>C</i>‐Glycosides”) from the Anomeric Acetates" @default.
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- W1970512935 doi "https://doi.org/10.1002/ejoc.200700181" @default.
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