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• W1997703374 abstract "This paper describes the development of a compromised single-stage microwave-assisted digestion condition for multi-element determination in fish samples by inductively coupled plasm: mass spectrometry using experimental designs. A Plackett–Burman design was carried out as a multivariate strategy to investigate the main effects of the following parameter on microwave-assisted nitric acid digestion: microwave irradiation time, ramp time, digestion temperature, microwave power limit and the addition of hydrogen peroxide or hydrochloric acid. The most significant microwave setting parameters (radiation time, ramp and temperature) were further evaluated by response surface methodology under Box–Behnken design, while others were kept constant. The influences of different parameters vary according to metal element, thus the working conditions were established as a compromise within optimum region found for each targeted element which ensures quantitative recoveries and time efficiency. The compromised condition..." @default.
• W1997703374 created "2016-06-24" @default.
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• W1997703374 date "2011-08-18" @default.
• W1997703374 modified "2023-09-24" @default.
• W1997703374 title "Evaluation of microwave-assisted digestion condition for the determination of metals in fish samples by inductively coupled plasma mass spectrometry using experimental designs" @default.
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• W1997703374 doi "https://doi.org/10.1080/03067319.2010.548093" @default.
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