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- W1997883142 abstract "[reaction: see text] The enantioselective synthesis of colletodiol has been achieved in 11 steps from methyl 1,3,5-octatrienoate and 16 total steps from both ethyl sorbate and methyl 1,3,5-octatrienoate. The route relies upon an enantio- and regioselective Sharpless dihydroxylation and a palladium-catalyzed reduction to form a 5-hydroxy-1-enoate and an 7-hydroxy-1,3-dienoate. These esters were further functionalized, coupled, and macrolactonized to provide colletodiol after deprotection. Grahamimycin A and colletol were synthesized in one and two steps, respectively, from colletodiol." @default.
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- W1997883142 date "2002-11-16" @default.
- W1997883142 modified "2023-09-23" @default.
- W1997883142 title "Enantioselective Syntheses of Colletodiol, Colletol, and Grahamimycin A" @default.
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- W1997883142 doi "https://doi.org/10.1021/ol0269502" @default.
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