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- W2014062456 abstract "When DSC is used in the isothermal mode to monitor exothermic reactions a horizontal baseline is usually assumed. The true non-linear baseline can be obtained from a second run on the fully reacted sample. This method was evaluated using the reaction of phenylglycidyl ether and 2-ethyl-4-methylimidazole in a 2:1 molar ratio. The assumption of horizontal baselines gives an apparently decreasing heat of reaction over the temperature range 80–151°C, while the use of experimentally determined non-linear baselines gives a constant heat of reaction, 459.7 J g−1 with standard deviation 17.3 J g−1." @default.
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- W2014062456 date "1983-12-01" @default.
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- W2014062456 title "An improved method for the use of DSC in the isothermal mode to monitor exothermic reactions" @default.
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- W2014062456 doi "https://doi.org/10.1016/0040-6031(83)80066-5" @default.
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