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- W2026473364 abstract "The reaction of [Rh(S2CNEt2)(CO)2] and HpzAn (3(5)-p-methoxyphenylpyrazole) in acetone at in room temperature yields to a mixture of [Rhu(μ-pzAn)(S2CNEt2)(CO)]2 (2) and [Rh(S2CNEt2)3] (3). The same results were obtained from the reaction of [RhCI(CO)2(H-pzAn)] with NaS2CNEt2. The first reaction in boiling solvents (acetone, dichloromethane) didn't yield to the binuclear complex (2) but an unexpected complex [Rh(S2CNEt2)(CO)]2 (1) was obtained. Complex (1) was proved to be the evolution result of the starting [Rh(S2CNEt2)(CO)2] in boiled solvents. The molecular structure of complex (3) has been determined. Crystals of (3) are monoclinic, space group C2/c, and is a different form than that previously reported for [Rh(S2CNEt2)3]. Subtle differences between the molecular structures are also found." @default.
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- W2026473364 date "1998-05-01" @default.
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- W2026473364 title "The reactivity of [Rh(S2CNEt2) (CO)2] towards HpzAn" @default.
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- W2026473364 doi "https://doi.org/10.1016/s0277-5387(97)00385-9" @default.
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