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- W2034546089 abstract "Plutonium tetranitrato complexes with N,N′-dialkyl monoamides A[A = dibutyl derivatives of hexanamide (DBHA), octanamide (DBOA)] and tetraalkyl diamides B [B = tetrabutyl, tetraisobutyl and tetrahexyl malonamide (TBMA, TIBMA, THMA)] have been isolated and characterized as Pu(NO3)4 · 3A and Pu(NO)3)4 · 2B, respectively. Complexes with diamides such as Pu(NO3)4 · 2TBMA and Pu(NO3)4 · 2TIBMA were isolated as solids while all others were viscous liquids. Uranyl dinitrato-amide complexes with the above monoamides and diamides were synthesized and characterized as UO2(NO3)2 · 2A and UO2(NO3)2 · B. The IR and visible absorption spectra of the plutonium and uranium complexes indicate that they are O-bonded and the nitrate group acts as a bidentate group. The NMR spectra of the uranyl monoamide complexes indicate the existence of restricted rotation around the CN bond, while thermal investigations reveal that decomposition proceeds through three exothermic steps corresponding to the release of amide and nitrate groups and finally leading to U3O8." @default.
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- W2034546089 date "1995-09-01" @default.
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- W2034546089 title "Synthesis and characterization of some new mono- and diamide complexes of plutonium(IV) and dioxouranium(VI) nitrates" @default.
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- W2034546089 doi "https://doi.org/10.1016/0277-5387(95)00078-7" @default.
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