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- W2042058747 abstract "A novel N -nitrosamine of cyclam has been synthesized. The N–N bond lengths values, as determined from the X-ray crystal structure, fall in the 1.318(2) and 1.320(2) A range, smaller than the ones expected for the N–N single bond. The N–NO bond angles are in the 115.0(1)° and 114.8(1)° range. The ν NO, ν NN, and δ N–NO vibrational modes were observed in the infrared spectrum at 1454, 1139, and 555 cm −1 , respectively. The photolysis of the cyclam(NO) 4 compound gives rise to the nitrosyl release through an heterolytic cleavage of the N–NO bonds, as indicated by the appearance of the ν NO + band at 2228 cm −1 at the expense of decreasing the ν NO, ν NN, and δ N–NO bands." @default.
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- W2042058747 date "2005-03-01" @default.
- W2042058747 modified "2023-09-26" @default.
- W2042058747 title "Synthesis, characterization, and structure of a new N-nitrosamine of cyclam (1,4,8,11-tetraazacyclotetradecane)" @default.
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- W2042058747 doi "https://doi.org/10.1016/j.tetlet.2005.01.097" @default.
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