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• W2046719332 abstract "A first structurally characterized primary aminophosphane (Ar2PNH2 (2); Ar = 2,4,6-iPr3C6H2) that is a stable solid at room temperature without decomposition by self-condensation is reported. Reactions of N-phosphanyllithium amide (tBu2PNHLi (3)) with Me2SiCl2 and MeSiCl3 in Et2O result in the formation of Me2Si(NHPtBu2)2 (4) and MeSi(NHPtBu2)3 (5), respectively. Subsequent treatment of 4 and 5 with 2 and 3 equiv of nBuLi gave the dilithium (6) and trilithium (7) complexes, respectively. Further treatment of 5 with 3 equiv of AlMe3 yielded the trialuminum complex MeSi[N(AlMe2)PtBu2]3 (8). These three complexes were investigated by microanalysis and multinuclear NMR spectroscopy. The dilithium complex [Me2Si(NLiPtBu2)2·3THF] (6) and the trilithium complex [MeSi(NLiPtBu2)3·3Et2O] (7) were further characterized by single-crystal X-ray structural analysis." @default.
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• W2046719332 date "2008-08-19" @default.
• W2046719332 modified "2023-10-18" @default.
• W2046719332 title "Functionalization of Aminophosphanes: Synthesis and X-Ray Crystal Structure of Novel Dilithium and Trilithium Complexes Containing Silicon-Fused Heteronuclear SiN₂PLi Five-Membered Rings" @default.
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• W2046719332 doi "https://doi.org/10.1021/ic800995h" @default.
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