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• W2052206911 abstract "In recent years, several workers have examined the utility of IR spectroscopy to probe in situ the specific adsorption of electrolyte anions at metal electrodes [1-10]. There is interest in examining the behavior of electrolyte anions at metal electrodes to gain an insight into the structure of the electrical double layer and its effect on electrochemical reactivity. An early series of IR experiments aimed at probing electrolyte adsorption examined the interaction of sulfate and bisulfate at polycrystalline platinum electrodes under aqueous electrochemical conditions [3-6]. These studies explored electrolyte adsorption over a wide range of electrode potential and solution pH values. Potential-dependent alterations in the position of sulfate and bisulfate spectral features were observed and the vibrational bands were assigned to modes of adsorbed surface species on the basis of the perturbations observed [3-6]. More recent IR experiments examined bisulfate adsorption at P t ( l l l ) over the double layer and hydrogen adsorption potential regions and reported bisulfate spectral perturbations similar to those obseryed in experiments that employed polycrystalline platinum [10]. Studies which aimed to define the practical analytical limits of the in situ IR technique have indicated the importance of considering the effect of potential-dependent alterations in the composition of the thin layer cavity on the appearance of the sulfate and bisulfate spectral features [7-9]. In the thin layer spectroelectro-" @default.
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• W2052206911 date "1993-06-01" @default.
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• W2052206911 title "IR spectroscope as a probe of bisulfate absorption at platinum electrodes under aqueous electrochemical conditions: elimination of bulk interference by using a thin layer flow cell" @default.
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• W2052206911 doi "https://doi.org/10.1016/0022-0728(93)80243-b" @default.
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