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- W2063503869 abstract "Synthesis and Characterization of Platinumcyclobutadiene Complexes by the Reduction of Hexachloroplatinic AcidHexachloroplatinic acid is reduced in 1-butanol in the presence of an alkyne R–C≡C–R′ (R, R′ = Me, Et, nPr) to give platinumcyclobutadiene complexes [PtCl2(C4R2R2′)] (1). H[PtCl3(CH3CH2CH=CH2)] (2) is an intermediate which is isolated as bis(triphenylphosphoranylidene)ammonium salt (PPN-salt) [PPN][PtCl3(CH3CH2CH=CH2)] (3). The molecular structure of [PtCl2(C4Et4)] (1b) shows in the solid state a planar cyclobutadiene ring with internal bond angles of 93(3) and 87(2)°. The Pt–C bond lengths are 208(2) and 210(2) pm. The ethyl groups are pushed out of the ring plane, away from the Pt atom, with an angle of 7(2)°." @default.
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- W2063503869 date "1993-11-01" @default.
- W2063503869 modified "2023-09-27" @default.
- W2063503869 title "Zur Synthese und Charakterisierung von Platincyclobutadien‐Komplexen durch Reduktion von Hexachloroplatinsäure" @default.
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- W2063503869 doi "https://doi.org/10.1002/cber.19931261108" @default.
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