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- W2068065411 abstract "An α-alkylidation of cyclopentanone was achieved in two reaction steps in an overall yield of 20 to 79% via a zinc chloride-catalyzed thioalkylation of the zinc enolate of methyl 2-oxocyclopentanecarboxylate (3) and subsequent saponification/desulfurization of the β-(phenylthio) ketone intermediates 5. For the saponification/desulfurization step DABCO proved to be the reagent of choice and superior to the use of alkali or magnesium halides." @default.
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- W2068065411 date "1994-09-02" @default.
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- W2068065411 title "Thioalkylation of Enolates, IV. α-Alkylidenecyclopentanones by α-Alkylidation of Methyl 2-Oxocyclopentanecarboxylate" @default.
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- W2068065411 doi "https://doi.org/10.1002/jlac.199419940908" @default.
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