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- W2333599775 abstract "A simple and rapid procedure for the determination of a small amount of lead in tin metal and tin-base babbitt metal has been studied by dithizone photometric method. Large amounts of Sn (with Sb and As) are volatilized off by dropping HBr into H2SO4 solution at 200230° as described in the preceding report. Using benzene in place of CCl4 or CHCl3 as a solvent of dithizone, only one extraction is effective by employing a solution with high pH as has been reported by Snyder. Other interfering elements in such alloys are masked by NH2OH, Rochelle salt, and KCN as usual; and Bi as an impurity is permissible. The procedure is carried out as follows : after dissolving the sample in H2SO4 and volatilizing off Sn, Sb, and As, the solution is evaporated nearly to dryness, taken up in a little HNO3. Then this solution is made up to a definite volume with water, the aliquot of the solution is treated with NH2OH and Rochelle salt, and made strongly ammonical. KCN is added and the Pb is extracted as above." @default.
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- W2333599775 date "1956-01-01" @default.
- W2333599775 modified "2023-10-04" @default.
- W2333599775 title "Spectrophotometric Determination of Lead in Tin Metal and Tin-Base Babbitt Metal with Dithizone" @default.
- W2333599775 doi "https://doi.org/10.2116/bunsekikagaku.5.442" @default.
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