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- W243045851 abstract "The AiResearch Casting Company baseline silicon nitride (92 percent GTE SN-502 Si/sub 3/N/sub 4/ plus 6 percent Y/sub 2/O/sub 3/ plus 2 percent Al/sub 2/O/sub 3/) was characterized with methods that included chemical analysis, oxygen content determination, electrophoresis, particle size distribution analysis, surface area determination, and analysis of the degree of agglomeration and maximum particle size of elutriated powder. Test bars were injection molded and processed through sintering at 0.68 MPa (100 psi) of nitrogen. The as-sintered test bars were evaluated by x-ray phase analysis, room and elevated temperature modulus of rupture strength, Weibull modulus, stress rupture, strength after oxidation, fracture origins, microstructure, and density from quantities of samples sufficiently large to generate statistically valid results. A series of small test matrices were conducted to study the effects and interactions of processing parameters which included raw materials, binder systems, binder removal cycles, injection molding temperatures, particle size distribution, sintering additives, and sintering cycle parameters." @default.
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- W243045851 date "1985-10-01" @default.
- W243045851 modified "2023-09-26" @default.
- W243045851 title "Improved silicon nitride for advanced heat engines. Annual Technical Report, 26 September 1984-30 September 1985" @default.
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