FRINK Linked Data Fragments server

Matches in SemOpenAlex for { <https://semopenalex.org/work/W2499684991> ?p ?o ?g. }

• W2499684991 abstract "Stevioside and rebaudioside A are major diterpene glycoside from Stevia rebaudiana. These compounds have similar structure and make both compounds have close polarity. The aim of this study was to improve isocratic RP-HPLC analysis to achieve a complete separation of stevioside and rebaudioside A in baseline peak. The method improved was conducted on Eurosphere C-18 (250 × 4.6 mm, 5 µm) as the stationary phase. Mobile phase was made by a mixture of water-methanol (90: 10, v / v, pH = 3.0); acetonitrile, and trifluoroacetic acid (TFA) in the ratio 65: 35: 0.01 (v/v/v). Flow rate of mobile phase was 0.6 mL/min. The detection was performed in UV-210 nm. The improved method has complete separation by R > 2.00 in baseline peak. The linearity of the standard curve was obtained with a correlation coefficient of 0.9998 for rebaudioside A and 0.9994 for stevioside. The percent recovery was determined by standard addition method with a mean recovery of 100.82% for rebaudioside A and 101.04% for stevioside. The relative standard deviation (RSD) of intraday precision varies from 0.34 – 1.79% for rebaudioside A and 0.31 – 1.81% for stevioside, and interday precision showed RSD 1.47% for rebaudioside A and 0.37% for stevioside. While the sensitivity reported in the limit of detection (LOD) value of method improvement was 1.00 µg/mL for both rebaudioside A and stevioside. The limit of quantitation (LOQ) of the method was 3.00 µg/mL for both respected compounds. The small changes of the mobile phase composition, the mobile phase is reused after 1 week, flow rate, and column temperature did not alter the method performance significantly. The reliable and robust of the developed and validated method was applied to both simple and complex matrices of samples including S. rebaudiana leaves for major diterpene glycoside analysis." @default.
• W2499684991 created "2016-08-23" @default.
• W2499684991 creator A5004120893 @default.
• W2499684991 creator A5023411591 @default.
• W2499684991 creator A5043281085 @default.
• W2499684991 creator A5078462002 @default.
• W2499684991 date "2016-01-01" @default.
• W2499684991 modified "2023-10-11" @default.
• W2499684991 title "Improvement method of fast and isocratic RP-HPLC analysis of major diterpene glycoside from Stevia rebaudiana leaves" @default.
• W2499684991 cites W1512312954 @default.
• W2499684991 cites W1964492320 @default.
• W2499684991 cites W1972477859 @default.
• W2499684991 cites W1981529791 @default.
• W2499684991 cites W1989454094 @default.
• W2499684991 cites W1990183583 @default.
• W2499684991 cites W2005742734 @default.
• W2499684991 cites W2006881644 @default.
• W2499684991 cites W2008805118 @default.
• W2499684991 cites W2010822261 @default.
• W2499684991 cites W2016369023 @default.
• W2499684991 cites W2019274430 @default.
• W2499684991 cites W2021379453 @default.
• W2499684991 cites W2022451308 @default.
• W2499684991 cites W2045724914 @default.
• W2499684991 cites W2048019575 @default.
• W2499684991 cites W2050344678 @default.
• W2499684991 cites W2050828597 @default.
• W2499684991 cites W2074226013 @default.
• W2499684991 cites W2089582529 @default.
• W2499684991 cites W2102810898 @default.
• W2499684991 cites W2324047018 @default.
• W2499684991 cites W2497735451 @default.
• W2499684991 doi "https://doi.org/10.1063/1.4958509" @default.
• W2499684991 hasPublicationYear "2016" @default.
• W2499684991 type Work @default.
• W2499684991 sameAs 2499684991 @default.
• W2499684991 citedByCount "5" @default.
• W2499684991 countsByYear W24996849912017 @default.
• W2499684991 countsByYear W24996849912018 @default.
• W2499684991 countsByYear W24996849912020 @default.
• W2499684991 countsByYear W24996849912022 @default.
• W2499684991 crossrefType "proceedings-article" @default.
• W2499684991 hasAuthorship W2499684991A5004120893 @default.
• W2499684991 hasAuthorship W2499684991A5023411591 @default.
• W2499684991 hasAuthorship W2499684991A5043281085 @default.
• W2499684991 hasAuthorship W2499684991A5078462002 @default.
• W2499684991 hasBestOaLocation W24996849911 @default.
• W2499684991 hasConcept C113196181 @default.
• W2499684991 hasConcept C119128265 @default.
• W2499684991 hasConcept C142724271 @default.
• W2499684991 hasConcept C179998833 @default.
• W2499684991 hasConcept C185592680 @default.
• W2499684991 hasConcept C194671627 @default.
• W2499684991 hasConcept C204787440 @default.
• W2499684991 hasConcept C2776577345 @default.
• W2499684991 hasConcept C2778379570 @default.
• W2499684991 hasConcept C2780365743 @default.
• W2499684991 hasConcept C2992134379 @default.
• W2499684991 hasConcept C31903555 @default.
• W2499684991 hasConcept C43617362 @default.
• W2499684991 hasConcept C71240020 @default.
• W2499684991 hasConcept C71924100 @default.
• W2499684991 hasConceptScore W2499684991C113196181 @default.
• W2499684991 hasConceptScore W2499684991C119128265 @default.
• W2499684991 hasConceptScore W2499684991C142724271 @default.
• W2499684991 hasConceptScore W2499684991C179998833 @default.
• W2499684991 hasConceptScore W2499684991C185592680 @default.
• W2499684991 hasConceptScore W2499684991C194671627 @default.
• W2499684991 hasConceptScore W2499684991C204787440 @default.
• W2499684991 hasConceptScore W2499684991C2776577345 @default.
• W2499684991 hasConceptScore W2499684991C2778379570 @default.
• W2499684991 hasConceptScore W2499684991C2780365743 @default.
• W2499684991 hasConceptScore W2499684991C2992134379 @default.
• W2499684991 hasConceptScore W2499684991C31903555 @default.
• W2499684991 hasConceptScore W2499684991C43617362 @default.
• W2499684991 hasConceptScore W2499684991C71240020 @default.
• W2499684991 hasConceptScore W2499684991C71924100 @default.
• W2499684991 hasLocation W24996849911 @default.
• W2499684991 hasOpenAccess W2499684991 @default.
• W2499684991 hasPrimaryLocation W24996849911 @default.
• W2499684991 hasRelatedWork W1981395996 @default.
• W2499684991 hasRelatedWork W2027587692 @default.
• W2499684991 hasRelatedWork W2050016947 @default.
• W2499684991 hasRelatedWork W2288392566 @default.
• W2499684991 hasRelatedWork W2534870996 @default.
• W2499684991 hasRelatedWork W2789976878 @default.
• W2499684991 hasRelatedWork W2795518442 @default.
• W2499684991 hasRelatedWork W2950259075 @default.
• W2499684991 hasRelatedWork W3115475123 @default.
• W2499684991 hasRelatedWork W4319295017 @default.
• W2499684991 isParatext "false" @default.
• W2499684991 isRetracted "false" @default.
• W2499684991 magId "2499684991" @default.
• W2499684991 workType "article" @default.