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• W3126172205 startingPage "1321" @default.
• W3126172205 abstract "This first asymmetric total synthesis of (+)-srilankenyne (1), a halogenated C15 tetrahydropyran acetogenin isolated from Aplysia oculifera, features a sequence-sensitive process guided by conformational analysis to solve the challenging problem of introducing halogens. A competing semipinacol rearrangement during the installation of C(12)-bromide was suppressed by our A1,3 strain-controlled bromination protocol with support from X-ray crystallographic and computational studies. The C(10)-chloride was then placed by the Nakata chloromesylate-mediated chlorination." @default.
• W3126172205 created "2021-02-15" @default.
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• W3126172205 date "2021-02-03" @default.
• W3126172205 modified "2023-10-16" @default.
• W3126172205 title "Asymmetric Total Synthesis and Determination of the Absolute Configuration of (+)-Srilankenyne via Sequence-Sensitive Halogenations Guided by Conformational Analysis" @default.
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• W3126172205 doi "https://doi.org/10.1021/acs.orglett.0c04303" @default.
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