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- W4214895918 abstract "Abstract This paper deals with the densification and phase transformation of Si 3 N 4 with additives of Li-exchanged zeolite during pressureless sintering at significantly reduced temperatures. Dilatometric shrinkage data show that the first liquid forms as low as 1080 °C. Upon sintering at 1500 °C the bulk density increases to more than 95% of the theoretical density without phase transformation from α-S 3 N 4 to β-Si 3 N 4 , i. e. the phase transformation lags behind the densification process. Above 1500 °C the secondary phase is completely converted into a glass and the α-to-β transformation takes place. Under these conditions the grain growth is anisotropic, leading to a microstructure which has potential for enhanced fracture toughness. The results show that a very effective low-temperature sintering additive for silicon nitride can be obtained from Li-exchanged zeolite." @default.
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- W4214895918 date "2006-09-01" @default.
- W4214895918 modified "2023-09-23" @default.
- W4214895918 title "Sintering of Si<sub>3</sub>N<sub>4</sub> with Li-exchanged zeolite additive" @default.
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- W4214895918 doi "https://doi.org/10.1515/ijmr-2006-0199" @default.
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