Matches in SemOpenAlex for { <https://semopenalex.org/work/W4283012034> ?p ?o ?g. }
- W4283012034 endingPage "107700" @default.
- W4283012034 startingPage "107700" @default.
- W4283012034 abstract "A novel hyper-crosslinked 2, 8, 14, 20-tetraphenyl calix [4] resorcinol arene polymer (HCP-TCRA) was synthesized by using an external crosslinking of 2, 8, 14, 20-Tetraphenyl calix [4] resorcinol arene (TCRA) as monomers and dimethoxymethane as crosslinker. The HCP-TCRA was explored as a SPME fiber coating material. A variety of physicochemical characterization demonstrated that the material has excellent chemical/thermal stability and strong hydrophobicity. The fiber demonstrated fantastic adsorptive property for three synthetic estrogens (diethylstilbestrol, hexestrol, ethinyloestradiol, abbreviated to SESs). In this work, an efficient HCP-TCRA fiber-based SPME method was developed to analyze SESs by coupling with HPLC-MS detection. Under the optimized SPME conditions, this method was shown a wide range of linearity (2.0–100.0 ng mL−1 for diethylstilbestrol, 1.0–100.0 ng mL−1 for hexestrol, and 30.0–480.0 ng mL−1 for ethinyloestradiol), low limits of detection (LODs, 0.5 ng mL−1 for DES 0.3 ng mL−1 for HEX, 10.0 ng mL−1 for EES) and fine reusability (more than 30 times). Finally, the proposed methods had been applied to the determination of SESs in milk samples with a simple pretreatment. At three different levels, relative recoveries presented between 86.7 and 106.4%. The method put up highly sensitive and budget-friendly in detection SESs, and has capacity in quality control of milk products." @default.
- W4283012034 created "2022-06-18" @default.
- W4283012034 creator A5014793897 @default.
- W4283012034 creator A5049088369 @default.
- W4283012034 creator A5054899321 @default.
- W4283012034 creator A5061873699 @default.
- W4283012034 creator A5068047224 @default.
- W4283012034 creator A5088696461 @default.
- W4283012034 date "2022-10-01" @default.
- W4283012034 modified "2023-09-25" @default.
- W4283012034 title "Determination of synthetic estrogens in milk by a novel hyper-crosslinked polymer SPME coupled with HPLC-MS" @default.
- W4283012034 cites W1968108385 @default.
- W4283012034 cites W1977376942 @default.
- W4283012034 cites W1979255022 @default.
- W4283012034 cites W1990040897 @default.
- W4283012034 cites W2002108923 @default.
- W4283012034 cites W2010157979 @default.
- W4283012034 cites W2014247706 @default.
- W4283012034 cites W2018386672 @default.
- W4283012034 cites W2037571397 @default.
- W4283012034 cites W2050137868 @default.
- W4283012034 cites W2050378905 @default.
- W4283012034 cites W2058807244 @default.
- W4283012034 cites W2059606344 @default.
- W4283012034 cites W2071181539 @default.
- W4283012034 cites W2074650088 @default.
- W4283012034 cites W2075446999 @default.
- W4283012034 cites W2078096677 @default.
- W4283012034 cites W2080893705 @default.
- W4283012034 cites W2082696606 @default.
- W4283012034 cites W2095046805 @default.
- W4283012034 cites W2235467996 @default.
- W4283012034 cites W2498670133 @default.
- W4283012034 cites W2514737452 @default.
- W4283012034 cites W2599098845 @default.
- W4283012034 cites W2726654265 @default.
- W4283012034 cites W2806964676 @default.
- W4283012034 cites W2912744998 @default.
- W4283012034 cites W2919262787 @default.
- W4283012034 cites W2979490278 @default.
- W4283012034 cites W3008938362 @default.
- W4283012034 cites W3040145221 @default.
- W4283012034 cites W3093218851 @default.
- W4283012034 cites W3173218300 @default.
- W4283012034 cites W3212217047 @default.
- W4283012034 cites W4211173318 @default.
- W4283012034 doi "https://doi.org/10.1016/j.microc.2022.107700" @default.
- W4283012034 hasPublicationYear "2022" @default.
- W4283012034 type Work @default.
- W4283012034 citedByCount "3" @default.
- W4283012034 countsByYear W42830120342023 @default.
- W4283012034 crossrefType "journal-article" @default.
- W4283012034 hasAuthorship W4283012034A5014793897 @default.
- W4283012034 hasAuthorship W4283012034A5049088369 @default.
- W4283012034 hasAuthorship W4283012034A5054899321 @default.
- W4283012034 hasAuthorship W4283012034A5061873699 @default.
- W4283012034 hasAuthorship W4283012034A5068047224 @default.
- W4283012034 hasAuthorship W4283012034A5088696461 @default.
- W4283012034 hasConcept C118792377 @default.
- W4283012034 hasConcept C119128265 @default.
- W4283012034 hasConcept C161790260 @default.
- W4283012034 hasConcept C162602672 @default.
- W4283012034 hasConcept C166595027 @default.
- W4283012034 hasConcept C178790620 @default.
- W4283012034 hasConcept C179998833 @default.
- W4283012034 hasConcept C185592680 @default.
- W4283012034 hasConcept C2779684741 @default.
- W4283012034 hasConcept C2780016452 @default.
- W4283012034 hasConcept C2780890875 @default.
- W4283012034 hasConcept C2781397067 @default.
- W4283012034 hasConcept C43617362 @default.
- W4283012034 hasConcept C519885992 @default.
- W4283012034 hasConcept C521977710 @default.
- W4283012034 hasConcept C55493867 @default.
- W4283012034 hasConcept C71315377 @default.
- W4283012034 hasConceptScore W4283012034C118792377 @default.
- W4283012034 hasConceptScore W4283012034C119128265 @default.
- W4283012034 hasConceptScore W4283012034C161790260 @default.
- W4283012034 hasConceptScore W4283012034C162602672 @default.
- W4283012034 hasConceptScore W4283012034C166595027 @default.
- W4283012034 hasConceptScore W4283012034C178790620 @default.
- W4283012034 hasConceptScore W4283012034C179998833 @default.
- W4283012034 hasConceptScore W4283012034C185592680 @default.
- W4283012034 hasConceptScore W4283012034C2779684741 @default.
- W4283012034 hasConceptScore W4283012034C2780016452 @default.
- W4283012034 hasConceptScore W4283012034C2780890875 @default.
- W4283012034 hasConceptScore W4283012034C2781397067 @default.
- W4283012034 hasConceptScore W4283012034C43617362 @default.
- W4283012034 hasConceptScore W4283012034C519885992 @default.
- W4283012034 hasConceptScore W4283012034C521977710 @default.
- W4283012034 hasConceptScore W4283012034C55493867 @default.
- W4283012034 hasConceptScore W4283012034C71315377 @default.
- W4283012034 hasFunder F4320322990 @default.
- W4283012034 hasFunder F4320323826 @default.
- W4283012034 hasLocation W42830120341 @default.
- W4283012034 hasOpenAccess W4283012034 @default.
- W4283012034 hasPrimaryLocation W42830120341 @default.
- W4283012034 hasRelatedWork W1964259887 @default.