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• W4381848914 abstract "Abstract We described here a simple and metal‐free protocol to synthesize [1,2,3]triazolo[1,5‐ a ]quinoline 3‐carboxamides through a two‐step synthetic strategy, in which the first step uses organocatalysis (10 mol % of diethylamine or 1,8‐diazabicyclo[5.4.0]undec‐7‐ene, while the second step involves the use of inorganic base (1.2 or 0.1 equiv. of potassium hydroxide). These reactions were performed between β ‐keto amides and o ‐carbonyl phenylazides in dimethylsulfoxide as solvent at 70 °C for 2 h. The synthetic protocol is ample, which thirteen examples of secondary [1,2,3]triazolo[1,5‐ a ]quinoline 3‐carboxamides were synthesized ranging from good to excellent yields (63‐96 %), and six different tertiary [1,2,3]triazolo[1,5‐ a ]quinolines 3‐carboxamides were obtained ranging from moderate to good yields (48–76 %)." @default.
• W4381848914 created "2023-06-25" @default.
• W4381848914 creator A5008881125 @default.
• W4381848914 creator A5018277960 @default.
• W4381848914 creator A5046977939 @default.
• W4381848914 creator A5047559937 @default.
• W4381848914 creator A5055579743 @default.
• W4381848914 creator A5056666876 @default.
• W4381848914 date "2023-07-11" @default.
• W4381848914 modified "2023-10-17" @default.
• W4381848914 title "Synthesis of [1,2,3]Triazolo[1,5‐<i>a</i>]quinoline‐3‐carboxamides Promoted by Organocatalyst and Base" @default.
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