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- W4385830151 abstract "In this study, silicide coatings were successfully prepared on Mo substrates using NaCl-KCl-NaF molten salt as the reaction medium and K 2 SiF 6 as the silicon source. The electrochemical reduction mechanism of Si(IV) was studied by cyclic voltammetry and chronoamperometry technology. The effect of reaction temperature on the phase composition, microstructure, and growth kinetics of the electrodeposited coatings were investigated in detail. The long-term oxidation behaviors of Mo and MoSi 2 -coated Mo samples at 873 K were also compared. The results revealed that the electrodeposition of silicide coatings was closely related to the reaction temperature. Dense and coherent single-layer MoSi 2 coatings could be obtained at 1023 K and 1073 K, while double-layer coatings with inner MoSi 2 layer and outer Si layer could be obtained at 1123 K. Under the same electrodeposition time, the overall thickness of the silicide coatings increased with the reaction temperature. Moreover, long-term oxidation tests at 873 K proved that MoSi 2 coatings could effectively prevent the Mo substrate from oxidation. The mass gain of the MoSi 2 -coated Mo sample was only 0.46 wt% after 500 h of oxidation, which could be attributed to the formation of the continuous SiO 2 protective layer." @default.
- W4385830151 created "2023-08-16" @default.
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- W4385830151 date "2023-08-01" @default.
- W4385830151 modified "2023-09-27" @default.
- W4385830151 title "Effect of Reaction Temperature on the Molten Salt Electrodeposition of Silicide Coating on Molybdenum Substrate and its Oxidation Behavior" @default.
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- W4385830151 doi "https://doi.org/10.1149/1945-7111/acf076" @default.
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