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- W92222817 abstract "Ochratoxin A (OTA) was determined in 274 samples of dry pasta sold across Canada in 2004 to 2006. Ground sample was extracted with acetonitrile-water (6:4 [vol/vol]), filtered, diluted with phosphate-buffered saline, and cleaned with an immunoaffinity column. Analysis was by reversed-phase liquid chromatography with fluorescence detection, and in the second year by liquid chromatography-electrospray tandem mass spectrometry as well. For 2004 and 2005, the limit of quantitation was approximately 0.5 ng of OTA per g (signal-to-noise ratio of 10:1). In 2006, the limit of quantitation was estimated to be 0.2 ng of OTA per g. Incidence of contamination above 0.5 ng of OTA per g was 21, 18, and 66% in the years 2004, 2005, and 2006, respectively, reflecting the contamination variability of durum wheat crops and showing the importance of multiyear surveillance. Mean levels of OTA found in these 3 years were, respectively, 0.30, 0.28, and 0.76 ng/g, and maximum levels were, respectively, 1.8, 1.4, and 3.3 ng/g." @default.
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- W92222817 date "2009-04-01" @default.
- W92222817 modified "2023-10-16" @default.
- W92222817 title "Survey of Dry Pasta for Ochratoxin A in Canada" @default.
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- W92222817 doi "https://doi.org/10.4315/0362-028x-72.4.890" @default.
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