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• W1978045170 abstract "Abstract A soluble polyamide was synthesized from aromatic and aliphatic monomers by condensing 4‐aminophenyl sulfone with sebacoyl chloride in dimethylacetamide (DMAc) at low temperature under inert atmosphere. A stoichiometric amount of triethylamine was added to precipitate the HCl produced during the polymerization reaction. The precipitates were isolated, yielding a clear neat polyamide solution. Thin and transparent film achieved from the polymer resin was characterized for FTIR, NMR, gel permeation chromatography (GPC), thermogravimetry, differential scanning calorimetry, water absorption, and mechanical measurements. The dried film was found to be soluble in DMAc, DMSO, and DMF. The film‐forming property of polyamide is being exploited for the preparation of the nanocomposites. Spectroscopic analyses confirmed the formation of polyamide. The values of M n , M w , and polydispersity as determined by GPC were found to be 9,779, 20,280 g/mol and 2.07 with RI detector whereas 10,133, 20,865 g/mol and 2.06 with UV detector, respectively. The thermally stable polyamide exhibited tensile strength (18.86 MPa), glass transition temperature (72.34°C), and water absorption (16.1%). These studies further verified the related physical properties of the polyamide. © 2010 Wiley Periodicals, Inc. Adv Polym Techn 29:300–308, 2010; View this article online at wileyonlinelibrary.com . DOI 10.1002/adv.20197" @default.
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• W1978045170 date "2010-11-16" @default.
• W1978045170 modified "2023-10-16" @default.
• W1978045170 title "Synthesis and characterization of soluble aromatic-aliphatic polyamide" @default.
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• W1978045170 doi "https://doi.org/10.1002/adv.20197" @default.
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