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- W2034190760 abstract "In this paper, we developed a hydrothermal method to fabricate sheet-like and pseudo-octahedral magnetite crystals. X-ray diffraction (XRD) confirmed the products were pure spinel-structured magnetite. Scanning electron microscopy (SEM) was used to investigate the morphology of the obtained crystals. By carefully regulating the initial NaOH concentrations, the morphology of the products could be changed from sheet-like crystals to pseudo-octahedral crystals. Transmission electron microscopy (TEM) analysis indicated the sheet-like crystals were the oriented aggregation of nanoparticles. Pseudo-octahedral magnetite crystals were single crystalline, and were obtained by dissolution–recrystallization of the sheet-like crystals. Vibrating sample magnetometer (VSM)) suggested the magnetic properties of the products were strongly related to the morphology. The coercivity of the sheet-like magnetite crystals was 100 Oe, larger than 30 Oe of the pseudo-octahedral crystals, but the saturation magnetization of the sheet-like magnetite crystals was 40 emu/g, smaller than 85 emu/g of the pseudo-octahedral crystals." @default.
- W2034190760 created "2016-06-24" @default.
- W2034190760 creator A5012678595 @default.
- W2034190760 creator A5079033119 @default.
- W2034190760 creator A5091087406 @default.
- W2034190760 date "2010-12-01" @default.
- W2034190760 modified "2023-09-23" @default.
- W2034190760 title "Hydrothermal synthesis of magnetite crystals: From sheet to pseudo-octahedron" @default.
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- W2034190760 doi "https://doi.org/10.1016/j.materresbull.2010.09.023" @default.
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