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• W2038458002 abstract "Four oxidation products formed during the allomerisation reaction of chlorophyll a in methanol have been separated and identified using normal phase high-performance liquid chromatography (NP-HPLC) coupled with atmospheric pressure chemical ionisation (APCI) tandem mass spectrometry (MS/MS) and photodiode array detection. Fragmentation pathways of the main stereoisomers of the four major products, Mg-purpurin-7 dimethyl phytyl ester, 15(1)-MeO-lact-chl a, 13(2)-MeO-chl a and 13(2)-HO-chl a, have been assigned using APCI-MS(n) aided by examination of deuteriated counterparts of the purpurin and the lactone. Diagnostic fragmentations have been determined, including those for Mg-purpurin-7 dimethyl phytyl ester and 15(1)-MeO-lact-chl a, which display very similar full MS and MS/MS spectra. The use of NP-HPLC offers a rapid and efficient method which, combined with MS/MS, reduces reliance on precursor ion mass for assignment of structure in the allomerisation reaction where major and minor components are often isobaric." @default.
• W2038458002 created "2016-06-24" @default.
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• W2038458002 date "2002-02-01" @default.
• W2038458002 modified "2023-10-09" @default.
• W2038458002 title "Atmospheric pressure chemical ionisation normal phase liquid chromatography mass spectrometry and tandem mass spectrometry of chlorophylla allomers" @default.
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• W2038458002 doi "https://doi.org/10.1002/rcm.597" @default.
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