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• W2045004638 abstract "(Perfluoroalkyl)(dimethylamino)sulfonium Hexafluoroarsenates MeN = S(CF3)2 (5) is alkylated by Me3O⊕ AsF⊖6 to Me2N-S(CF3)⊕2 AsF⊖6 (4). From 5 and MeOSO⊕ AsF⊖6 (6) MeOS(O)-N(Me)S(CF3)⊕2 AsF⊖6 (7) is formed as a relatively stable primary product. Decomposition of 7 gives the expected 4 only in poor yield. Nucleophilic substitution of the sulfur-bonded fluorine in CF3SF⊕2 AsF⊖6 (8) by Me3SiNMe2 yields CF3S(NMe2)⊕2 AsF⊖6 (9). Similarly, (CF3)2CFSF⊕2 AsF⊖6 (10) reacts with dimethyl(trimethylsilyl)amine to give (CF3)2CFS(NMe2)⊕2 AsF⊖6 (11). The structures of 4 and 9 are elucidated by X-ray analyses, and the influence of the substituents on the bonding is discussed." @default.
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• W2045004638 date "1991-01-01" @default.
• W2045004638 modified "2023-09-27" @default.
• W2045004638 title "(Perfluoralkyl)(dimethylamino)sulfonium‐hexafluoroarsenate" @default.
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• W2045004638 doi "https://doi.org/10.1002/cber.19911240106" @default.
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