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• W2057029083 abstract "A multi-residue method is described that eliminates the need for a clean-up step and thus allows the rapid determination of pesticides in crude extracts of lettuce. Samples were extracted with a mixture of ethyl acetate, Na2SO4 and NaHCO3 and the crude extracts analysed directly using large volume-difficult matrix introduction (LV-DMI) in combination with gas chromatography-time of flight-mass spectrometry (GC-TOF-MS). The LV-DMI procedure described was evaluated for the analysis of dimethoate, pyrimethanil, chlorothalonil, vinclozolin, furalaxyl and oxadixyl. Satisfactory response was obtained at the lowest calibrated level (LCL) of 0.0025 microg ml(-1), with good linearity over the range 0.0025-0.5 microg ml(-1) (0.005-1.0 mg kg(-1) equivalent). Average recoveries between 73 and 118% were obtained at the 0.01-0.5 mg kg(-1) levels with RSD values < or = 13%." @default.
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• W2057029083 date "2003-01-01" @default.
• W2057029083 modified "2023-10-14" @default.
• W2057029083 title "Analysis of pesticide residues in lettuce by large volume–difficult matrix introduction–gas chromatography–time of flight–mass spectrometry (LV-DMI-GC-TOF-MS)" @default.
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• W2057029083 doi "https://doi.org/10.1039/b306482d" @default.
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