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• W2062804597 endingPage "9934" @default.
• W2062804597 startingPage "9931" @default.
• W2062804597 abstract "There is much current interest in nanostructured materials (nanotubes, nanobelts, nanospheres, etc.). Their crystal structures can differ from those of the equivalent bulk materials. Determining these differences is important in understanding how the properties of nanomaterials differ from those of the bulk. Established methods of X-ray structure determination become increasingly difficult or impossible to apply on reducing the dimensions to a few nanometers. Here we show that, by combining the Debye equation for X-ray scattering (which relates an ensemble of atoms to their diffraction pattern without recourse to symmetry) with a model of the crystal structure, generated by folding the ideal crystal structure into a nanotube, the severely broadened/distored powder diffraction pattern may be described. This procedure reveals the significant structural deformations necessary to accommodate the nanotube shape. The importance of knowing the (deformed) crystal structure is discussed." @default.
• W2062804597 created "2016-06-24" @default.
• W2062804597 creator A5056496930 @default.
• W2062804597 creator A5084117896 @default.
• W2062804597 date "2008-07-01" @default.
• W2062804597 modified "2023-09-25" @default.
• W2062804597 title "Demonstrating Structural Deformation in an Inorganic Nanotube" @default.
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• W2062804597 doi "https://doi.org/10.1021/ja8028334" @default.
• W2062804597 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/18593127" @default.
• W2062804597 hasPublicationYear "2008" @default.
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