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• W2070299436 abstract "A convenient, multikilogram-scale, stereoselective process for the synthesis of (1R,4S)-4-(3,4-dichlorophenyl)-1,2,3,4-tetrahydronaphthalen-1-amine hydrochloride 1 is described. The key steps involve synthesis of sulfinyl imine (Rs,4S)-5 from (S)-tetralone (4S)-3 and (R)-tert-butylsulfinamide (Rs)-4, and its stereoselective reduction with 9-BBN to produce the (1R)-amine center of 1. The process has been scaled up to multikilogram scale and gives 1 in an overall yield of >50% with a chemical purity of 99.7 A% by HPLC and stereochemical purity of >99.9% by chiral HPLC." @default.
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• W2070299436 date "2007-06-20" @default.
• W2070299436 modified "2023-10-13" @default.
• W2070299436 title "Development of a Large-Scale Stereoselective Process for (1<i>R</i>,4<i>S</i>)-4-(3,4-Dichlorophenyl)-1,2,3,4-tetrahydronaphthalen-1-amine Hydrochloride" @default.
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• W2070299436 doi "https://doi.org/10.1021/op7000589" @default.
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