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• W2080492956 endingPage "1996" @default.
• W2080492956 startingPage "1987" @default.
• W2080492956 abstract "A novel redox active (E,E)-dioxime ligand, S,S′-bis-[2(2′-ferrocenemethylaminobenzyl)]-dithioglyoxime (LH2), containing ferrocene and flexible aminobenzenesulfanyl-moieties on the periphery has been synthesized from 2-(2′-ferrocenemethylamino)benzenethiol, which was obtained by the reduction of 2,2′-pyridylbenzothiazolidine with a large excess of NaBH4. Mononuclear (LH)2M (M=NiII, CuII, CoII, FeII and MnII), homodinuclear (LH)2(UO2)2(OH)2 and heterotrinuclear (LH)2MM2′Xn (M=NiII and M′=PdII, X=Cl−, n=4 and M′=AgI, X=NO3 −, n=2) complexes have been obtained with the metal:ligand ratios of 1:2, 2:2 and 3:2, respectively. Flexible ferrocenemethylaminobenzenesultanyl moieties bearing two different heteroatoms, –S and –N, on the periphery of the vic-dioxime serve as weak binding sites for PdII and AgI ions. The detection of H-bonding in all complexes except the uranyl complex by IR revealed square-planar MN4 coordination of the mono- and trinuclear complexes. The MN4 coordination of the NiII complex was also determined by the 1H NMR spectroscopy. The structures of the complexes were characterized by elemental analysis, 1H NMR, IR, MS, UV–Vis spectral and cyclic voltammetry. The voltammetric analyses of the complexes showed metal, ligand, and ferrocene based signals. The redox chemistry of the complexes exhibited both MI and MIII oxidation states of the central metals of the complexes." @default.
• W2080492956 created "2016-06-24" @default.
• W2080492956 creator A5015441512 @default.
• W2080492956 creator A5034893854 @default.
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• W2080492956 date "2004-07-01" @default.
• W2080492956 modified "2023-09-26" @default.
• W2080492956 title "A new redox-active multisite ligand: synthesis, spectroscopy and electrochemistry of its mono and dinuclear complexes, and the interaction of (E,E)M (M=Ni) complex with PdII and AgI" @default.
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• W2080492956 doi "https://doi.org/10.1016/j.poly.2004.05.009" @default.
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