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• W2088892180 abstract "Abstract New heterodinuclear Zn II /Ni II ( 1 ) and homodinuclear Ni II /Ni II ( 2 ) water-soluble and air stable compounds of general formula [M(H 2 O) 6 ][M′(dipic) 2 ] ·  m H 2 O have been easily prepared by self-assembly of the corresponding metal(II) nitrates with dipicolinic acid (H 2 dipic) in water solution at room temperature.  The compounds have been characterized by IR, UV/Vis and atomic absorption spectroscopies, elemental and X-ray single crystal diffraction (for 1  · 4H 2 O and 2  · 5H 2 O) analyses.  3D infinite polymeric networks are formed via extensive hydrogen bonding interactions involving all coordinated and crystallization water molecules, and all dipicolinate oxygens, thus contributing to additional stabilization of dimeric units, metal-organic chains and 2D layers.  In 1  · 4H 2 O, the latter represent a rectangular-grid 2D framework with multiple channels if viewed along the c crystallographic axis, while in 2  · 5H 2 O intercalated crystallization water molecules are associated to form acyclic nonplanar hexameric water clusters and water dimers which occupy voids in the host metal-organic matrix, with a structure stabilizing effect via host–guest interactions.  The hexameric cluster extends to the larger (H 2 O) 10 one with an unusual geometry (acyclic helical octamer with two pendent water molecules) by taking into account the hydrogen bonds to water ligands in [Ni(H 2 O) 6 ] 2+ .  The obtained Zn/Ni compound 1 relates to the recently reported family of heterodimetallic complexes [M(H 2 O) 5 M′(dipic) 2 ] ·  m H 2 O (M/M′ = Cu/Co, Cu/Ni, Cu/Zn, Zn/Co, Ni/Co, m  = 2, 3), what now allows to establish the orders of the metal affinity towards the formation of chelates with dipicolinic acid (Co II  > Ni II  > Zn II  > Cu II ) or aqua species (Co II II II II )." @default.
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• W2088892180 date "2008-05-01" @default.
• W2088892180 modified "2023-09-25" @default.
• W2088892180 title "3D hydrogen bonded metal-organic frameworks constructed from [M(H2O)6][M′(dipicolinate)2] ·mH2O (M/M′ = Zn/Ni or Ni/Ni). Identification of intercalated acyclic (H2O)6/(H2O)10 clusters" @default.
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• W2088892180 doi "https://doi.org/10.1016/j.ica.2006.12.016" @default.
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