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• W2090118489 abstract "Since the prediction of Liu and Cohen [Science 245, 841 (1989)] of the potential extraordinary mechanical properties of crystalline β-C3N4, many authors have attempted its synthesis. However, in most cases, the obtained materials are amorphous phases with a complex bonding structure. Their characterization is complicated due to the absence of a reference compound, the lack of long-range order, and the poor knowledge about their bonding structure. In this article, we present H1, C13, and N15 solid-state nuclear magnetic resonance (NMR) measurements for the determination of the bonding types in amorphous CNx films. NMR measurements do not require long-range order and are able to clearly identify the signals from the sp2- and sp3-bonded phases. The analysis of the data obtained by other characterization techniques, such as infrared spectroscopy, x-ray photoelectron spectroscopy, electron energy-loss spectroscopy, and x-ray absorption near-edge spectroscopy on the same sample, based on the information acquired by NMR, enables the description of a structure model for the studied amorphous-CNx phase prepared by dc-magnetron sputtering and to revise the interpretation found in the literature." @default.
• W2090118489 created "2016-06-24" @default.
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• W2090118489 date "2001-07-15" @default.
• W2090118489 modified "2023-10-16" @default.
• W2090118489 title "Bonding structure in amorphous carbon nitride: A spectroscopic and nuclear magnetic resonance study" @default.
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• W2090118489 doi "https://doi.org/10.1063/1.1380998" @default.
• W2090118489 hasPublicationYear "2001" @default.
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