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• W2130367050 abstract "Abstract Radical polymerizations of di‐ n ‐butyl itaconate were investigated. Unexpected resonances (C resonances) were observed in 13 C NMR spectra of CO of poly(di‐ n ‐butyl itaconate)s [poly(DBI)s] obtained at temperatures higher than 60 °C, although two kinds of carbonyl groups showed splittings due to triad tacticities in the spectra of polymers obtained at lower temperatures. The poly(DBI)s formed by the different kinds of initiators or formed in the presence of chain‐transfer agents showed hardly any changes in the intensities of the C resonances; this indicated that the C resonances were not due to the structures formed through initiating and terminating reactions. The poly(DBI)s obtained at different yields showed only a slight increase in the intensities of the C resonances with the yield, which suggested that the C resonances were not attributable to the intermolecular chain‐transfer reaction to the monomer and/or polymer. However, the intensities of the C resonances significantly increased with a decreasing feed monomer concentration; this suggested that intramolecular chain‐transfer reactions took place at high temperatures. Furthermore, a Cu complex‐catalyzed atom transfer radical polymerization mechanism was revealed to be effective for suppressing the intramolecular chain‐transfer reaction at 60 °C. © 2002 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 40: 2415–2426, 2002" @default.
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• W2130367050 date "2002-05-30" @default.
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• W2130367050 title "Chain-transfer reaction in the radical polymerization of di-n-butyl itaconate at high temperatures" @default.
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• W2130367050 doi "https://doi.org/10.1002/pola.10316" @default.
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