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- W2477029216 abstract "In this paper, synthesis and characterization of two type morphologies of the MCM-41mesoporous material, nano and microfibers, were investigated by electrospinning technique. The synthesis was performed in acidic and alkaline media, separately. The MCM-41 morphologies were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM), x-ray powder diffraction (XRD), and nitrogen adsorption–desorption measurement. Tetraethylorthosilicate (TEOS) and cetyltrimethylammonium bromide (CTAB) were used as silica and template sources for the synthesis of MCM-41 morphologies, respectively. The SEM results showed that MCM-41 nanofibers were spun in acidic media and microfibers of MCM-41 were produced in alkaline media. The XRD study revealed a long range structural ordering of mesoporous materials. The TEM results indicated rough surfaces with uniform average diameter 200 nm for nanofibers and 2 µm for microfibers. The pore diameter and surface area of calcined MCM-41 nanofibers were 2.2 nm and 970 m2/g, respectively. For the MCM-41 microfibers, pore sizes of 2.7 nm and surface areas 420 m2/g was measured." @default.
- W2477029216 created "2016-08-23" @default.
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- W2477029216 date "2016-10-01" @default.
- W2477029216 modified "2023-10-16" @default.
- W2477029216 title "Fabrication of MCM-41 fibers with well-ordered hexagonal mesostructure controlled in acidic and alkaline media" @default.
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- W2477029216 doi "https://doi.org/10.1016/j.jssc.2016.07.030" @default.
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