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- W100041384 abstract "Abstract The reaction of H 2 with 13 CO adsorbed on Pd/Al 2 O 3 has been investigated by solid state 13 C NMR. As the reaction proceeds, the peak for adsorbed CO on the Pd particles decreases while the intensity of a new peak near 60 ppm increases. This new peak is tentatively assigned to methoxy groups. When the sample was annealed at temperatures higher than 180°C, gas phase CH 4 was observed as a sharp peak near -10 ppm. The metallic character of the Pd particles was studied by observing the first moment and spin lattice relaxation time of the 13 CO on Pd which changed as the reaction progressed. Proton NMR was also employed to confirm the assignment of 13 C peaks as well as the presence of palladium hydride." @default.
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- W100041384 date "1993-01-01" @default.
- W100041384 modified "2023-09-30" @default.
- W100041384 title "Methoxy formation/spillover on Pd/Al2O3 studied by 13C, 1H NMR" @default.
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- W100041384 doi "https://doi.org/10.1016/s0167-2991(08)63179-1" @default.
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