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- W1007998464 abstract "以自制的Pd—Fe/TiO2为催化剂,对3-氟-4-硝基苯酚常压催化加氢得到3-氟-4-氨基苯酚,用熔点、元素分析、IR和^1H NMR对他们的结构进行了表征,证明为目标产物;确定优化工艺条件为:0.1mol硝基物,催化剂0.26g,无水乙醇作溶剂,用量为60mL,反应温度为40℃,0.1MPa下加氢反应3h,产率为98.6%,产物的纯度达99.2%。" @default.
- W1007998464 created "2016-06-24" @default.
- W1007998464 creator A5003832822 @default.
- W1007998464 creator A5065392280 @default.
- W1007998464 date "2007-12-25" @default.
- W1007998464 modified "2023-09-23" @default.
- W1007998464 title "用Pd-Fe/TiO2常压催化加氢合成3-氟-4-氨基苯酚的研究" @default.
- W1007998464 hasPublicationYear "2007" @default.
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