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- W1010705226 abstract "A novel thiopyrano(4,3-d)pyrimidine derivative compound 1 was synthesized with methyl dimethyl 3,3'-thiodipropionate as starting material through five steps, including cyclization, chlorination, substitution with morpholine and coupling with 5-bromopyridin-2-amine through S uzuki reaction. And its structure was confirmed by 1 H NMR and MS. The total yield of the five steps was 18.6% (calculated from methyl dimethyl 3,3'-thiodipropionate).Compound 1 is an important intermediate in the design and synthesis of thiopyrano(4,3-d)pyrimidine derivatives small molecule inhibitors.Therefore, the synthesis of Compound 1 has an important significance in the the study of anticancer drugs." @default.
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- W1010705226 date "2015-01-01" @default.
- W1010705226 modified "2023-09-25" @default.
- W1010705226 title "Synthesis of 5-(4-Morpholino-7, 8-dihydro-5H-thiopyrano[4,3-d]pyrimidin-2-yl)pyridin-2-amine" @default.
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- W1010705226 doi "https://doi.org/10.2991/emim-15.2015.168" @default.
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