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• W1013078492 abstract "A new analytical strategy was developed that integrates a generic sample preparation into a liquid chromatography–multistage ion trap/time-of-flight mass spectrometry (LC-IT(MSn)/TOF), allowing for large-scale screening and qualitative confirmation of wide-scope illegal adulterants in different food matrices. Samples were pretreated by a fast single-tube multifunction extraction for accurate multistage mass measurement on the hybrid LC-IT/TOF system. A qualitative validation performed for over 500 analyte–matrix pairs showed the method can reduce most of the matrix effects and achieve a lower limit of confirmation at 0.1 mg/kg for 73% of the target compounds. A unique combination of dual-polarity detection, retention time, isotopic profile, and accurate MSn spectra enables more comprehensive and precise confirmation, based on the multiparameter matching by automated library searching against the user-created database. Finally, the applicability of this LC-IT(MSn)/TOF-based screening procedure for discriminating coeluting isobars, identifying nontarget adulterants, and even tentatively elucidating unexpected species in real samples is demonstrated." @default.
• W1013078492 created "2016-06-24" @default.
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• W1013078492 date "2015-07-31" @default.
• W1013078492 modified "2023-09-27" @default.
• W1013078492 title "Wide-Scope Screening of Illegal Adulterants in Dietary and Herbal Supplements via Rapid Polarity-Switching and Multistage Accurate Mass Confirmation Using an LC-IT/TOF Hybrid Instrument" @default.
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• W1013078492 doi "https://doi.org/10.1021/acs.jafc.5b02222" @default.
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