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- W103458531 abstract "A simple, rapid, and accurate method for the estn. of thiosemicarbazide (TSC) alone and in its metal complexes (with Zn, Cd, Hg, Ni, Pt, and Pd) in aq. medium, based on oxidn. with excess chloramine-B and back titrn. of the excess chloramine-B iodometrically, was developed. The oxidn. involves a 12-electron stoichiometry per TSC mol. in aq. medium of pH 2-7 and in the presence of 0.1N mineral acids. The proposed anal. method is useful for the rapid estn. of the ligand on a macroscale and also for computing the no. of ligand mols. in a TSC-metal complex. [on SciFinder(R)]" @default.
- W103458531 created "2016-06-24" @default.
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- W103458531 date "1981-01-01" @default.
- W103458531 modified "2023-09-27" @default.
- W103458531 title "Sodium N-chlorobenzenesulfonamide (chloramine-B) as an analytical reagent: estimation of thiosemicarbazide alone and in its metal complexes." @default.
- W103458531 hasPublicationYear "1981" @default.
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