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- W1042012177 abstract "A new multimonomer, the poly[2-(4-pentenoyloxy)ethyl methacrylate] (PPEM) has been synthesized by Schotten-Bauman's esterification of poly(2-hydroxyethyl methacrylate) with 4-pentenoyl chloride. Its chemical structure wasconfirmed by means of FTIR, 1 H NMR, 1 3 C NMR spectra as well as by elemental analysis. Differential scanning calorimetry (DSC) and thermogravimetry (TG) were used to determine the thermal behavior of the PPEM. It was seen, that thermal polymerization of side vinyl groups and thermal decomposition of the multimonomer appear within the 247-380°C range (under nitrogen). Introduction of 1 wt. % of AIBN under nitrogen reduces PPEM polymerization temperature to 136°C. PPEM undergoes photopolymerization at room temperature to crosslinked products." @default.
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- W1042012177 date "2002-11-01" @default.
- W1042012177 modified "2023-09-24" @default.
- W1042012177 title "Preparation and characterization of poly[2-(4-pentenoyloxy)ethyl methacrylatel" @default.
- W1042012177 doi "https://doi.org/10.14314/polimery.2002.813" @default.
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