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• W1141820188 abstract "Publisher Summary This chapter describes the results of the investigations on an interface for coupling supercritical fluid chromatography (SFC) with inductively coupled plasma-atomic emission spectrometric (ICP-AES) of different design from those developed for high performance liquid chromatography (HPLC-ICP) and FIA (flow injection analysis)-ICP. In SFC-ICP interfacing the signal intensity measured by ICP is strongly dependent on chromatographic conditions. Therefore, effects of the chromatographic conditions in SFC on the emission signal intensity is investigated using the pseudocolumn under chromatographic conditions as like so-called supercritical FIA analysis. The advantage of changing modifiers in SFC-ICP is most significant when the analytes span a wide molecular weight/polarity range. Since the total effluent enters the ICP torch, quantitation should be straightforward. Also, it is expected that background signal changes due to organic modifiers are small. The chapter further discusses the separation of organometallic conditions. The results of the investigations demonstrate that the SFC-ICP system is an effective tool for speciation of metal-containing compounds, even when the modifiers are added to the supercritical carbon dioxide mobile phase to control the retention of components. An advantage of microcolumn SFC-ICP hyphenation described in this chapter results from the significantly reduced flow rates of microcolumns compared with those of conventional columns, due to the reduced amount of effluents which enter the ICP." @default.
• W1141820188 created "2016-06-24" @default.
• W1141820188 creator A5067776339 @default.
• W1141820188 date "1992-01-01" @default.
• W1141820188 modified "2023-09-27" @default.
• W1141820188 title "Chapter 9 Inductively Coupled Plasma Atomic Emission Spectrometric Detection in Supercritical Fluid Chromatography" @default.
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• W1141820188 doi "https://doi.org/10.1016/s0301-4770(08)61231-2" @default.
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