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- W1170078533 abstract "The triclinic phase of zinc molybdate α-ZnMoO4 (ZMO) was synthesized by a simple co-precipitation method at 600 °C. The crystal structure of the obtained polycrystalline sample of ZMO was characterized by X-ray diffraction (XRD) and Rietveld calculations using the space group P-1. The electrical properties of α-ZnMoO4 compacted pellets were determined at room temperature from electrical impedance spectrometry (EIS), in the temperature range of 400–700 °C. Nyquist representations were interpreted in terms of two types of electrical circuits, involving a high frequency bulk component and a low frequency Warburg component. Analyses of the frequency dependence of the real and imaginary impedance show a non-Debye type relaxation. A phase transition corresponding to the allotropic transformation triclinic–monoclinic (α→β) of ZnMoO4 was observed in the temperature range of 450–500 °C, with a variation of activation energies. The Warburg component is discussed in terms of electrode surface reactions." @default.
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- W1170078533 date "2015-12-01" @default.
- W1170078533 modified "2023-09-30" @default.
- W1170078533 title "Rietveld refinements, impedance spectroscopy and phase transition of the polycrystalline ZnMoO4 ceramics" @default.
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- W1170078533 doi "https://doi.org/10.1016/j.ceramint.2015.08.094" @default.
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