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- W1175324900 abstract "A new binucleating macrocyclic ligand 2,6-bis (1,4,7,10-te-traazacyclododecan-10-ylmethyl)methoxy-benzene (L) and its binuclear copper (II) complex, [ Cu2LBr2 ] (ClO4 )2 · 3H2O (1), was prepared and the structure was determined by X-ray crystallography. Complex 1 crystallizes in monoclinic crystal system, P21/n space group with a = 0.8206(3), b = 2.0892(8), c = 2.3053(7) nm, β=95.83(2)°, V = 3.932 nm3, Mr = 1017.57, Z = 4, Dc= 1.692 g/cm3, and R = 0. 0489, Rw= 0.0552 for 6571 observed reflections with I≥2σ (I). Both of the copper(II) centers are coordinated by four amine nitrogen donors of cyclen subunits and a bromide an-ion, and each copper (II) ion is in a square-pyramidal coordination environment. Variable temperature magnetic susceptibility studies indicate that there exists weak intramolecular an-tiferro-magnetic coupling ( - 2J = 2.06 cm-1) between the two copper(n) centers." @default.
- W1175324900 created "2016-06-24" @default.
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- W1175324900 date "2000-01-01" @default.
- W1175324900 modified "2023-09-24" @default.
- W1175324900 title "Synthesis, crystal structure and magnetic properties of the binuclear copper (II) complex of a new bis (1, 4, 7,10-tetraazacy-clodoclecane) ligand" @default.
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