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- W117775560 abstract "The effects of firing atmosphere and temperature on the yield of U(C,O) phase were investigated. Firing temperatures between 1000 and 2000 deg C were used as well as the following atmospheres: argon, carbon monoxide, mixtures of argon and carbon monoxide and argon and carbon dioxide, and vacuum. X-ray diffraction techniques were used to determine the phases present, the relative amounts of each phase, and the lattice parameters of the face centered cubic phases. When carbon monoxide or a partial pressure of either carbon dioxide or carbon monoxide with argon was used at temperatures between 1000 and 2000 deg C, reactions with uranium chips and uranium carbide occurred yielding UO/sub 2/, UC/ sub 2/, and UC or U(C,O). With these atmospheres no reaction was detected with UO/sub 2/ up to 1800 deg C. Therefore it is unlikely that U (C,O) free of other phases can be produced by reacting uranium or uranium carbide with carbon monoxide or carbon dioxide. However, use of very low partial pressures of carbon monoxide and/or carbon dioxide may produce the desired results. As processing techniques were improved, it became increasingly difficult to produce the U(C,O) phase with a lattice parameter of 4.950A which was the phasemore » selected for further investigation. This indicated that impurities are important in the formation of this phase. (auth)« less" @default.
- W117775560 created "2016-06-24" @default.
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- W117775560 date "1962-10-31" @default.
- W117775560 modified "2023-09-23" @default.
- W117775560 title "STUDY OF PHASE RELATIONSHIPS IN THE U-C-O SYSTEM. Progress Report, December 1961" @default.
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