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• W123575148 abstract "The physical and chemical nature of chemically bonded phases used in high performance liquid chromatography have been studied. These bonded phases were characterized by a variety of chromatographic and non-chromatographic experiments. The non-chromatographic techniques 13 included C NMR and batch extraction methods. The role played by the bonded as well as the mobile in determining the retention characteristics of the stationary phase were determined. The retention of solute molecules on bonded phases was found to be a function of the chain length of the bonded phase, the chemical nature of the bonded molecule, and the type of organic modifier used in the mobile phase. The energetics of the solute-stationary inter­ actions was determined by the differential enthalpy and was found to be indicative of a partitioning process between two liquid phases. The retention process was also affected by the surface coverage of the bonded molecule. Optimum retention and separation characteristics were obtained with a hydrocarbon bonded of high surface coverage when used with a mobile containing a very polar organic modifier. The efficiency of these bonded phases was found to be indepen­ dent of chain length as well as surface coverage of the bonded molecule. Some bonded phases which have specific functionalities incorporated into the bonded molecule are not true reversed phases." @default.
• W123575148 created "2016-06-24" @default.
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• W123575148 date "1980-01-01" @default.
• W123575148 modified "2023-09-27" @default.
• W123575148 title "THE CHARACTERIZATION OF BONDED PHASES FOR HIGH PERFORMANCE LIQUID CHROMATOGRAPHY" @default.
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