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• W1240192389 abstract "We present 11 B and 17 O magic-angle spinning (MAS) and multiple quantum (MQMAS) nuclear magnetic resonance (NMR) data for crystalline strontium tetraborate (SrB 4 O 7 ) and the glass with corresponding SrO·2B 2 O 3 composition. Crystalline SrB 4 O 7 contains a tricluster oxygen site (3 BO 4 neighbors) and can be used as a model compound for observing tricluster oxygen sites in the corresponding glass. NMR site parameters for the tricluster are distinguishable from those of the bridging oxygen atoms in SrB 4 O 7 , allowing for visible areas in the 17 O spectrum attributed solely to the presence of tricluster oxygen atoms. By overlapping the spectra of the crystalline SrB 4 O 7 and the corresponding glass there are indications for a maximum of a few percent of tricluster oxygen atoms within the glass. This is further confirmed by calculations of expected non-bridging oxygen (NBO) content without triclusters, done using 11 B MAS NMR and analyzed composition, in comparison to directly measured NBO content in the SrO·2B 2 O 3 glass, which suggests that up to 2% of the total oxygen atoms within this glass are in triclusters. • Crystalline strontium tetraborate (SrB 4 O 7 ) was compared to SrO·2B 2 O 3 glass. • 17 O NMR can directly detect tricluster oxygen sites in crystalline SrB 4 O 7 . • 11 B and 17 O NMR spectra suggest possibility of a few percent triclusters in glass. • Tricluster oxygen atoms in glass are also seen indirectly, from non-bridging oxygen contents. • Up to 2% of total oxygen atoms in SrO·2B 2 O 3 glass are tricluster oxygen atoms." @default.
• W1240192389 created "2016-06-24" @default.
• W1240192389 creator A5006383663 @default.
• W1240192389 creator A5057546665 @default.
• W1240192389 date "2015-11-01" @default.
• W1240192389 modified "2023-10-16" @default.
• W1240192389 title "Tricluster oxygen atoms in crystalline and glassy SrB4O7: High resolution 11B and 17O nuclear magnetic resonance analysis" @default.
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• W1240192389 doi "https://doi.org/10.1016/j.jnoncrysol.2015.08.014" @default.
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