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- W125280299 abstract "The electrochemistry of thionyl chloride was studied at glassy-carbon electrodes in dimethylformamide with tetrabutylammonium hexafluorophosphate as supporting electrolyte. Techniques employed were normal and reverse pulse voltammetry, rotating ring-disk voltammetry, coulometry and nuclear magnetic resonance. The reactions taking place during the reduction of thionyl chloride in dimethylformamide are probably best represented by the solvation reaction, SOCl/sub 2/ + 2DMF yields SO.2DMF(2+) + 2 Cl(-) and the electrochemical reaction, SO.2DMF(2+) + 2e yields SO where the product, SO, may be solvated by DMF and can be reoxidized back to the initial reactant." @default.
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- W125280299 date "1988-03-28" @default.
- W125280299 modified "2023-09-23" @default.
- W125280299 title "Electrochemical studies of sulfur oxychlorides. Final report, June 1983-December 1987" @default.
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