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- W1264542606 abstract "Abstract This research is devoted to microwave assisted combustion synthesis of Mo 2 C nanoparticles. The ternary system of MoO 3 –Zn–C was used as a novel approach for the in-situ synthesis of Mo 2 C in which the zincothermic reduction of MoO 3 was responsible for the combustion to take place. Results showed that the formation of Mo 2 C was assisted by the zincothermic reaction, although further microwave heating up to 6 min was necessary to complete the reaction. The effects of the microwave heating and mechanical activation on the reaction progress were investigated. X-ray powder diffraction was used to examine the synthesis progress. Final products (Mo 2 C and ZnO) were successfully separated from each other and the synthesized carbide was characterized by transmission electron microscopy (TEM), showing the formation of Mo 2 C hexagonal nanocrystals during combustion process." @default.
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- W1264542606 date "2015-10-01" @default.
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- W1264542606 title "On the formation of Mo2C nanocrystals by a novel system through microwave assisted combustion synthesis" @default.
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- W1264542606 doi "https://doi.org/10.1016/j.matchar.2015.08.015" @default.
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