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- W13071819 abstract "Methods are described for the determination of C in Pu metal, alloys, oxides, and carbides, together with a method for the separation of free C from combined C in thc PuC. In all cases the C is converted to CO/sub 2/ by combustion at high temperature in a stream of O. The CO/sub 2/ evolved is measured either manometrically by means of its pressure in a known volume or gravimetrically after absorption on soda asbestos. The manometric method is used for amounts of C in the range 25 Vg to 2 mg with a preciston (coefficient of variation) of 5% at the lower level and l.5% at the higher level. The gravimetric method is employed for samples containtng more C than can be esttmated by the manometric apparatus. The precision obtatnable ms therefore decided by the weighing techntque and for the determination of 27 mg of C is 0.5% (coefficient of variation). The free C in a sample of PuC is separated by taking advantage of the chemical reactivity of the combined C and dissolving this in C hydrochloric acid, leaving behind the uncombined C. The free C is then separated by filtration and determtned manometrically after combustion to CO/submore » 2/. (auth)« less" @default.
- W13071819 created "2016-06-24" @default.
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- W13071819 date "1961-09-01" @default.
- W13071819 modified "2023-09-24" @default.
- W13071819 title "THE DETERMINATION OF CARBON IN PLUTONIUM METAL ALLOYS, OXIDES AND CARBIDES" @default.
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